碳?xì)涞蜓醴治鰞x FLASH 2000

碳?xì)涞蜓醴治鰞x FLASH 2000  采用*的“動態(tài)閃燒 - 色譜分離分析”技術(shù)。只需要極小的進(jìn)樣量即可獲得C、H、S、N和O五種元素的精確含量。由于采用成熟的色譜分析技術(shù)，其樣品燃燒分解氣體采用一根內(nèi)徑極細(xì)的元素分析轉(zhuǎn)同填充柱分離， *避免了由于采用大量吸附劑而存在的殘留效應(yīng)，使得分析結(jié)果有很好的重現(xiàn)性和精度。特別適合分析任務(wù)較重、樣品數(shù)量較多的實驗室。 　 應(yīng)用范圍： · 環(huán)境監(jiān)控 混合肥料、廢棄物、軟泥、淤泥、礦泥、煤泥、沉淀物、肥料、殺蟲劑和木料 · 化學(xué)和藥物產(chǎn)品 精細(xì)化工產(chǎn)品、藥物產(chǎn)品、爆炸物、催化劑、有機金屬化合物、聚合物、合成橡膠、纖維材料和紡織產(chǎn)品 · 石油化工和能源 煤炭、石墨、焦碳、原油、燃料油、石油、汽油添加劑、潤滑油、油品添加劑 · 物理性質(zhì) 水泥、陶瓷、玻璃纖維、輪胎、燃料、色素、建筑材料 　 主要特點： 1．功能強大的軟件內(nèi)置了多種計算方法，（K因子法、線性回歸、非線性方程等）。 2．軟件具有強大的控制功能，儀器自動開機、關(guān)機、意外情況自動保護(hù)等，自動提示更換催化劑和反應(yīng)管。 3．儀器采用*的電子流量控制系統(tǒng)控制載氣和氧氣的流速。待機狀態(tài)下，將氦氣的流速降至10ml/min，并斷開O2的流速，可大大延長催化劑的使用壽命。 4．儀器反應(yīng)管的連接采用技術(shù)，不需要工具，可以方便地安裝和拆卸，反應(yīng)管以清理燃燒殘渣貨更換催化劑。 5．其分析結(jié)果不僅可以給出數(shù)據(jù)表格，還可以給出各元素的色譜峰，使結(jié)果更加直觀。 6．可根據(jù)實際要求選配33-125位估計自動進(jìn)樣器，或99為液體自動進(jìn)樣器。 7．儀器除了通用的CHSNO五元素模式外，另有CHN & O, NCS, CHN, CHNS, S等多種分析模式的配置。

 詳見：www.amcabj.com

有機/無機化學(xué)及醫(yī)藥領(lǐng)域 Organic/Inorganic Chemistry & Pharmaceuticals
• 精細(xì)化工 Fine Chemicals
• 制藥 Pharmaceuticals Products
• Organo-metallic compounds
• Polymers
• Plastic
• Synthetic rubbers
• Fibers
• Explosives
• Catalysts
• Textiles
• Pesticides
• Detergents
• Fluorine-compounds

材料特征分析鑒定領(lǐng)域 MATERIAL CHARACTERIZATION
• Glue/Resins
• Papers
• Rubbers
• Cement
• Ceramics
• Carbon/Glass Fibers
• Tires
• Pigments & Dyes
• Refractory materials
• Building materials
• Inorganic materials
• Metals
• Textile fibers
• Wood powders

環(huán)境分析領(lǐng)域 ENVIRONMENTAL ANALYSIS
• Soils, sediments,rocks
• Composts
• Wastes
• Sewage/sludge
• Pesticides
• Water solution
• Waste Water
• Particulates in Air by Filters
• Particulates in Water by Filters
• Woods

農(nóng)學(xué)與海洋生物領(lǐng)域 AGRONOMY & MARINE SCIENCE
• Soil
• Plants (leaves, roots, fruit)
• Sediments
• Humus
• Algae
• Plankton
• Particulate matter in water by filters
• Water
• Fertilizer

石油化學(xué)與能源領(lǐng)域 PETROCHEMISTRY & ENERGY
• Coals
• Cokes
• Crude oils
• Gasoline/Diesel
• Alternative fuels
• Petroleum derivates
• Lubricants
• Oil additives
• Graphite

人類學(xué)及動物學(xué)樣品分析領(lǐng)域 HUMAN & ANIMAL SAMPLES
• Blood
• Hairs
• Nails
• Serum
• Urine
• Faeces

同位素分析領(lǐng)域 ISOTOPE ANALYSIS
• Soilplant research
• Forensic
• Bio Oceanography
• Foodgoods control

 

Organic Materials
N % C % H % S %
dl-Methionine 9.41 40.24 7.43 21.42
RSD% 0.39 0.29 0.32 0.49
Theoretical value 9.39 40.25 7.43 21.49
BCR 71 10.86 40.55 2.32 8.18
RSD% 0.495 0.236 0.51 0.88
Theoretical value 10.85 40.39 2.37 8.30
BCR 72 9.647 36.13 2.078 7.344
RSD% 0.35 0.09 0.40 0.91
Theoretical Value 9.65 36.13 2,10 7.35
Sample weight: 2 – 3 mg
No. of analysis: 10
BCR 71: N-(4-bromophenyl)-N’-(2-chloro-4-nitrophenyl) thiourea
BCR 72: N-(2-chloro-4-nitrophenyl)-N’-(2-iodophenyl) thiourea
Petrochemistry
N % C % H % S % O % G.H.V. N.H.V.
South African
Coal 1.1 68.35 4.89 0.212 16.38 7293.55 7042.81
RDS% 0.35 0.09 0.40 0.91 0.847 0.34 0.33
Coke 2.183 89.4 3.266
RSD% 1.17 0.38 0.83
Sample weight: 2 – 3 mg
No. of analysis: 10
G.H.V. : Gross Heat Value (Kcal / Kg)
N.H.V. : Net Heat Value (Kcal / Kg)
Material Characterization
N % C % H % S %
Tyres A 0.5738 84.7714 7.8326 1.9753
RSD% 0.7299 0.2059 0.1743 0.9279
Tyres B 0.4796 89.9350 7.9260 0.8812
RSD% 0.5214 0.2234 0.1647 1.8431
Sample weight: 2 – 3 mg
No. of analysis: 10
Environmental Analysis
N % C % H % S % 0 %
Compost A 1.5401 40.8423 5.6829 0.4959 34.22
RSD% 1.994 0.153 0.3352 1.8353 0.6612
Compost B 1.8553 39.859 5.1919 0.583 31.352
RSD% 2.298 0.5687 0.6349 2.1293 0.5657
Sample weight: 3 – 4 mg
No. of analysis: 5

Sulfur determination by FPD (Flame Photometric Detector)
S ppm Average S ppm RSD % 
                  59
Clay          61 61 4.103
                  64 
                  12
Cellulosa 13 12 4.681 
                  12
Standard: Thermo Fisher Scientific Soil Reference Material (S: 320 ppm)
Standard weight: 1.5 – 5 mg
Sample weight : 2 – 3 mg
Note: the samples have been analyzed with the addition of 5 mg V2O5
Validation
Nowadays many companies must comply with extensive industry
government regulations.
Thermo Fisher is proud to recognise the Thermo Scientific
FLASH 2000 Series as the first OEA instrument equipped with a
specific qualification package. This package consists of extensive
documentationtailored validation kit(s) according to the
instrument configuration (CHNS, CHN, O etc.).
The FLASH 2000 Series Validation Package includes:
Declaration of Conformity
Equipments & Determination Profile
Qualifications:
IQ Installation Qualification / OQ Operational Qualification /
PQ Performance Qualification
Declaration of System Validation
Test results
Validation certificate

 

• 具備高度的靈活性，適用于各種領(lǐng)域 High flexibility to meet any requirement 
＊ Flash Combustion
The FLASH 2000 Series Analyzer operates according to the dynamic flash combustion (modified Dumas method) of the sample for the determination of Carbon, Hydrogen, NitrogenSulfur. Samples - organic or inorganic, solid or liquid – are weighed in a tin capsuleintroduced into the combustion reactor by an autosampler. When the sample enters the reactor, inserted in the special furnace heated at 900 – 1000°C, a small volume of pure Oxygen is added to the systemhelps to burn the organic or inorganic material, converting the sample into elemental (simple) gases. A separation columnTCD detector allows the user to determine element concentrations without using a complex splitting system, aliquote dosing device or purge & trap adsorbers. On the same instrument, but working in a different analytical condition, the Oxygen determination can be obtained when operating in pyrolysis mode. Utilizing the Flash Dynamic Combustion method, the FLASH 2000 Series achieves accurateprecise
sample characterization within a few minutes.
＊ Approved by official organizations
The Dynamic Flash Combustion technique is endorsed by a large array of renowned international official organizations including AOAC (Association of Official Analytical Chemists), AOCS (American Oil Chemists Society), AACC (American Association of Cereal Chemists), ASTM (American Society  for TestingMaterials)ASBC (American Society of Brewing Chemists). The simplicity of the method, unparalleled data reproducibilitytruly quantitative results are the essence of this wide acceptance.

• 于OEA的綜合能力強大的 Eager Xpreience 軟件 Eager Xperience software:
The most comprehensive software dedicated to OEA
The dedicated software controls the operation, data acquisitiondata evaluation capabilities of the FLASH 2000 Series enabling quick reference to method parametersinstrument status readout. Users can configure this flexible platform to gain access to either all available features or alternatively to a customizedsimplified user interface incorporating pre-set methods. Eager Xperience is the most advanced,
completeflexible dedicated software for OEA applications.

• 經(jīng)優(yōu)化操作運行，適用費用低 Optimized operation for lower cost
＊ Thermo Scientific OxyTune™ –Automatic Oxygen Dosing System
＊ Minimized maintenance downtime